Prepn: Crooks in The
Chemistry of Penicillin (Princeton Univ. Press, 1949)
p 470; Sheehan et al.,US2477148 and US2496416 (1949, 1950, both to Merck
& Co.).
Derivative
dl-Form.
Properties
Crystals from hot water, mp 183°.
Derivative
d-Form.
Properties
Crystals from water, mp 189-190°; [α]D25 +18° (50% ethanol).