Nomenclature
CAS number: 517-10-2
(3β)-Cholest-4-en-3-ol; coprostenol; 4:5-coprosten-3-ol.
C
27H
46O; mol wt 386.65.
C 83.87%, H 11.99%, O 4.14%.
Description and references
Prepn: Windaus, Ann. 453, 101 (1927); Schoenheimer, Evans, J. Biol. Chem. 114, 567 (1936).
Sepn from cholesterol: Stoll, Z. Physiol.
Chem. 246, 10 (1937).
Properties
Needles from ether-methanol, mp 132°. [α]D23 +43.7° (c = 1 in
benzene). Freely sol in benzene, acetone, ether, chloroform,
dioxane, pyridine; less sol in methanol, alcohol. Pptd by digitonin.
Deep-red color with 90% trichloroacetic acid.Derivative
Acetate.
C
29H
48O
2; mol wt 428.69.
C 81.25%, H 11.29%, O 7.46%.
Properties
Long needles from dil methanol, mp 85°.