Nomenclature
CAS number: 539-30-0
(Ethoxymethyl)benzene.
C
9H
12O; mol wt 136.19.
C 79.37%, H 8.88%, O 11.75%.
Description and references
Preparation from sodium ethoxide and benzyl
bromide: Letsinger, Pollart, J. Am. Chem.
Soc. 78, 6079 (1956); by reduction of benzaldehyde
diethyl acetal with LiAlH4-AlCl3: Eliel, Rerick, J. Org. Chem. 23, 1088 (1958).
Properties
Oily liquid, aromatic odor. bp 186°; bp10 65°. d 0.949, nD20 1.4955.
Volatile with steam. Practically insol in water; miscible with alcohol,
ether.