Nomenclature
CAS number: 105-46-4
Acetic acid 1-methylpropyl ester; acetic acid
sec-butyl ester.
C
6H
12O
2; mol wt 116.16.
C 62.04%, H 10.41%, O 27.55%.
Description and references
Prepd from sec-butanol and acetic
anhydride: R. Altschul, J. Am. Chem. Soc. 68, 2605 (1946). Prepn of d- and l-form: J. Kenyon et al., J. Chem.
Soc. 1935, 1072. Manuf: Faith, Keyes & Clark's Industrial Chemicals, F. A.
Lowenheim, M. K. Moran, Eds. (Wiley-Interscience, New York, 4th ed.,
1975) pp 171-177.
Derivative
dl-Form.
Properties
Liquid. d27 0.865. bp761 111-111.5°. nD27 1.3848. Flash pt, open cup: 88°F (31°C). Slightly sol in water; sol in
alcohol, ether.Derivative
d-Form.
Nomenclature
CAS number: 66610-38-6
Acetic acid (1
S)-1-methylpropyl ester.
Properties
[α]546.118 +10.52° (neat).Derivative
l-Form.
Nomenclature
CAS number: 54657-08-8
Acetic acid (1
R)-1-methylpropyl ester.
Properties
Liquid, bp 116-117°. d419 0.873. [α]546.119 -20.19° (neat). [α]546.119 -18.86° (c = 5.046 in ethanol). nD18 1.3899.Caution
Potential symptoms of overexposure
are irritation of eyes; headache; drowsiness; narcosis; dryness of
upper respiratory system and skin. See NIOSH Pocket Guide to Chemical Hazards (DHHS/NIOSH
97-140, 1997) p 38.