Nomenclature
CAS number: 109-73-9
1-Butanamine; 1-aminobutane.
C
4H
11N; mol wt 73.14.
C 65.69%, H 15.16%, N 19.15%.
Description and references
Prepn by reduction of butyraldoxime: Lycan et al., Org. Synth. coll. vol. II, 319 (1943). Usually manuf by catalytic alkylation
of ammonia with butyl alcohol: Davies et al., US 2609394 (1952 to I.C.I.); Hindley, Fisher, US 2782237 (1957 to British Celanese); Lemon, Myerly, US 3022349 (1962 to Union Carbide); Shirley, Speranza, US 3128311 (1964 to Jefferson Chem.). Manuf
from butyraldehyde and ammonia in the presence of Raney nickel: Brimer et al., US 2518659 (1950 to Eastman Kodak). Toxicity study: C.
H. Hine et al., Arch. Environ.
Health 1, 343 (1960).
Properties
Liquid, ammoniacal odor, bp 78°. mp -50°. d425 0.7327. nD20 1.4010.
Flash pt, open cup:
30°F (-1°C). Flammable,
corrosive. Misc with water, alcohol, ether. LD50 orally in rats:
500 mg/kg (Hine).Caution
Potential symptoms of overexposure
are irritation of eyes, skin, nose and throat; headache; skin flushing
and burns. See NIOSH Pocket Guide
to Chemical Hazards (DHHS/NIOSH 97-140, 1997) p 40.Use
Intermediate for pharmaceuticals, dyestuffs, rubber
chemicals, emulsifying agents, insecticides, synthetic tanning agents.