Nomenclature
CAS number: 18700-78-2
1,2,3,4-Tetrahydro-1,3,4,5,10-pentahydroxy-2-methyl-3-[(3-methyloxiranyl)carbonyl]-4a,9a-epoxyanthracen-9(10
H)-one; 4a,9a-epoxy-3-(2,3-epoxybutyryl)-1,2,3,4,4a,9a-hexahydro-1,3,4,5,10-pentahydroxy-2-methylanthrone.
C
19H
20O
9; mol wt 392.36.
C 58.16%, H 5.14%, O 36.70%.
Description and references
Antineoplastic antibiotic produced by Streptomyces ogaensis: Okuma et al., J. Antibiot. 15A, 152, 247 (1962).
Prepn: Sumiki et al., JP 64 7400 (1964 to Inst. Phys. & Chem. Res.). Structure: Marumo et al., J. Am. Chem. Soc. 86, 4507 (1964); eidem, Agric. Biol. Chem. 32, 209 (1968). Stereochemistry: eidem, ibid. 35, 1931 (1971). Activity
studies: C. Itakura et al., J.
Antibiot. 16A, 231 (1963).
Properties
Needles, mp 203-205° (dec). [α]D20 -144° (in ethanol). uv max: 227, 264, 323 nm (ε 14200, 7800, 2600). pKa 9.0. Sol in acetone, lower
alcohols, acetic acid, pyridine. Moderately sol in ethyl acetate,
ethyl ether, chloroform, carbon tetrachloride. Slightly sol in water,
benzene. Insol in petr ether, ligroin. Stable in neutral or acidic
soln; unstable in alkaline soln. LD50 i.p. in mice: 48.5 mg/kg (Itakura).