Nomenclature
CAS number: 36653-82-4
1-Hexadecanol; ethal; ethol; palmityl alcohol.
C
16H
34O; mol wt 242.44.
C 79.27%, H 14.14%, O 6.60%.
Description and references
Discovered by Chevreul in 1813. Obtained from
spermaceti by saponification: Spada, Gavioli, Farm. Sci. Tec. (Pavia) 7, 435 (1952), C.A. 47, 891c (1953). Prepn from
palmitoyl chloride + NaBH4: Caikin, Brown, J. Am. Chem. Soc. 71, 122 (1949);
from methylthiopalmitate + Raney Ni: Ruzicka, Prelog, US 2509171 (1950 to Ciba); from hexadecyl bromide: Levine, Clippinger, US 3018308 (1962 to California Res. Corp.).
Properties
White crystals. d 0.811. mp 49°. bp 344°; bp15 190°.
nD79 1.4283. Practically insol in water.
Sol in alcohol, chloroform, ether.Derivative
Hexadecyl alcohol.
Description and references
Primary, branched chain, C16 alcohol,
made up of an array of isomeric compds maintained in constant proportion
by a complex manufacturing process (not from spermaceti): Edman,
Lowden, Drug Cosmet. Ind. 93, 631 (Nov. 1963).
Properties
Liquid, d2020 0.842. bp50 195-205°. Freezes at <-60°.
Miscible with most alcohols, glycols, esters, ketones, cosmetic oils
and aromatics. Immiscible with water.Use
In cosmetics as emollient, emulsion modifier, coupling
agent. Pharmaceutic aid (emulsifying and stiffening agent).