Description and references
Prepn of monohydrate: Balthis, Jr., Bailar,
Jr., Inorg. Synth. 1, 122 (1939); Hatfield, ibid. 3, 148 (1950); Kranz, Witkowska, ibid. 6, 144 (1960); Ocone, Block, ibid. 8, 125 (1966). Toxicity study: H.
F. Smyth et al., Am. Ind. Hyg.
Assoc. J. 30, 470 (1969).
Derivative
Monohydrate.
Properties
Deep red powder, or monoclinic crystals; composed
of dimeric units. Easily oxidized, especially when moist, to chromic
acetate. Loses H2O when dried over P2O5 at 100°, changing color to brown. d 1.79. Slightly sol in cold water; readily
sol in hot water; sol in and reacts with most acids; slightly sol
in alcohol. Practically insoluble in ether. Keep tightly closed. LD50 orally in rats: 11.26 g/kg (Smyth). absorber
in gas analysis.