Nomenclature
CAS number: 93-51-6
2-Methoxy-4-methylphenol; 2-methoxy-
p-cresol; 4-methylguaiacol; 3-methoxy-4-hydroxytoluene; 4-hydroxy-3-methoxy-1-methylbenzene.
C
8H
10O
2; mol wt 138.16.
C 69.55%, H 7.30%, O 23.16%.
Description and references
Occurs in beechwood tar. It is one of the
active constituents of creosote. Obtained by the Clemmensen reduction
of vanillin using amalgamated zinc and toluene as auxiliary solvent:
Fletcher, Tarbell, J. Am. Chem. Soc. 65, 1431 (1943); Schwarz, Hering, Org. Synth. coll. vol. IV, 203 (1963).
Properties
Colorless to yellowish, strongly refractive, aromatic
liq. d425 1.092. bp760 220°; bp15 105°; bp4 79°. mp 5.5°. nD25 1.5353. Slightly sol in water; miscible
with alcohol, benzene, chloroform, ether, glacial acetic acid.Note
Not to be confused with cresol.