3122. Diethylmagnesium

Nomenclature

CAS number: 557-18-6
Magnesium diethyl.
C4H10Mg; mol wt 82.43.
C 58.28%, H 12.23%, Mg 29.49%.
Mg(C2H5)2.

Description and references

Prepd by the action of magnesium metal on mercury diethyl in ether: Schlenk, Jr., Ber. 64, 734, 736 (1931).

Properties

Solvated crystals from ether, MgEt2.Et2O, plates, rods. mp 0°. Liquid at room temp. Spontaneously flammable in air. Violent explosion on contact with water. Loses its ether of crystn on heating in vacuo. Not volatile in high vac up to 250° when decompn sets in. Sol in ether. Dec by alc and ammonia. Will glow and catch fire even in CO2. Must be handled in high vac, or under dry nitrogen or hydrogen.