3482. Dysprosium

Nomenclature

CAS number: 7429-91-6

Description and references

Dy; at. wt 162.500; at. no. 66; valences 2, 3, 4. A lanthanide; belongs to the yttrium group of rare earth metals. Naturally occurring isotopes (mass numbers): 156 (0.06%); 158 (0.10%); 160 (2.34%); 161 (18.9%); 162 (25.5%); 163 (24.9%); 164 (28.2%); known artificial radioactive isotopes: 145-155; 157; 159; 165-167. Abundance in earth's crust: ≈4.5 ppm. Occurs in gadolinite, xenotime, samarskite and other rare earth minerals. Discovered in 1886 by Lecoq de Boisbaudran. Sepn: Urbain, Compt. Rend. 139, 736 (1904); 141, 521 (1905); 142, 785 (1906); Spedding et al., J. Am. Chem. Soc. 69, 2812 (1947); 76, 2557 (1954). Prepn of salt: Engle, Balke, ibid. 39, 53 (1917); prepn of a Dy-Al alloy: Schumacher, Harris, ibid. 48, 3108 (1926). Toxicity studies: Bruce et al., Toxicol. Appl. Pharmacol. 5, 750 (1962); Haley et al., ibid. 8, 37 (1966). Reviews of prepn, properties and compds: The Rare Earths, F. H. Spedding, A. H. Daane, Eds. (Krieger, Huntington, N.Y., 1971, reprint of 1961 ed.) 641 pp; Hulet, Bode, “Separation Chemistry of the Lanthanides and Transplutonium Actinides” in MTP Int. Rev. Sci.: Inorg. Chem., Ser. One vol. 7, K. W. Bagnall, Ed. (Univ. Park Press, Baltimore, 1972) pp 1-45; Moeller, “The Lanthanides” in Comprehensive Inorganic Chemistry vol. 4, J. C. Bailar, Jr. et al., Eds. (Pergamon Press, Oxford, 1973) pp 1-101; F. H. Spedding in Kirk-Othmer Encyclopedia of Chemical Technology vol. 19 (John Wiley & Sons, New York, 3rd ed., 1982) pp 833-854; Chemistry of the Elements, N. N. Greenwood, A. Earnshaw, Eds. (Pergamon Press, New York, 1984) pp 1423-1449. Brief review of properties: G. T. Seaborg, Radiochim. Acta 61, 115-122 (1993).

Properties

Silver metal; tarnishes in moist air. Hexagonal close-packed crystals. d 8.5500. mp 1412°. bp 2567°. Heat of fusion: 10.782 kJ/mol. Heat of sublimation (25°): 290.4 kJ/mol. Forms greenish-yellow salts.

Derivative

Oxide.

Nomenclature

Dysprosia.
Dy2O3; mol wt 373.00.
Dy 87.13%, O 12.87%.

Properties

White substance. Prepd by heating the oxalate or sulfate. d27 7.81.

Derivative

Hydroxide.
Dy(OH)3; mol wt 213.52.
Dy 76.11%, O 22.48%, H 1.42%.

Properties

A gelatinous precipitate. Prepd by adding ammonia to an aq soln of a dysprosium salt; forms a blue colloidal soln.

Derivative

Chloride.
DyCl3; mol wt 268.86.
Dy 60.44%, Cl 39.56%.

Properties

Obtained by passing S2Cl2 over heated dysprosia. A hexahydrate is formed from the aq soln. The anhydr chloride, yellow shining crystals, d 3.67; mp 680°. LD50 in mice: 585 mg/kg i.p.; 7.65 g/kg orally (Haley).

Derivative

Sulfate.
Dy2(SO4)3; mol wt 613.19.
Dy 53.00%, S 15.69%, O 31.31%.

Properties

Octahydrate, yellow crystals. Prepd by dissolving the oxide in sulfuric acid and precipitating with alcohol; stable in air at 110°, dehydrated at 360°.

Derivative

Nitrate.
Dy(NO3)3; mol wt 348.51.
Dy 46.63%, N 12.06%, O 41.32%.

Properties

Pentahydrate, melts at 88.6° in its water of crystn. Sol in water. LD50 (hexahydrate) in rats: 295 mg/kg i.p.; 3.1 g/kg orally (Bruce).

Use

Oxide used in control rods of some nuclear power reactors.