Prepn: Synerholm, Zimmerman, Contrib. Boyce Thompson Inst. 14, 91 (1945); Templeman, Sexton, Proc. Roy. Soc. 133B, 300 (1946); Foster, GB 573479 and GB 573510 (both 1945 to ICI); Skeeters, US 2740810 (1956 to Diamond Alkali). Toxicity study: Rowe, Hymas, Am. J. Vet. Res. 15, 622 (1954). Review of carcinogenic risk: IARC Monographs 30, 255-269 (1983); of genotoxicity studies: B. Elliott, Mutagenesis 20, 3-13 (2005).