Nomenclature
CAS number: 7786-34-7
3-[(Dimethoxyphosphinyl)oxy]-2-butenoic acid methyl ester; 3-hydroxycrotonic acid methyl ester dimethyl phosphate; 1-methoxycarbonyl-1-propen-2-yl dimethyl phosphate; methyl 3-(dimethoxyphosphinyloxy)crotonate;
O,O-dimethyl 1-carbomethoxy-1-propen-2-yl phosphate; 2-carbomethoxy-1-methylvinyl dimethyl phosphate; ENT-22374; OS-2046; Phosdrin (AMVAC).
C
7H
13O
6P; mol wt 224.15.
C 37.51%, H 5.85%, O 42.83%, P 13.82%.
Description and references
Organophosphate insecticide; cholinesterase
inhibitor. Commercial product is a mixture of isomers, containing ≈60%
of the more active (E)- (also referred to as cis-) isomer. Prepn: A. R. Stiles, US 2685552 (1954 to Shell). Activity: R. A. Corey et al., J. Econ. Entomol. 46, 386 (1953); of isomers: J. E. Casida et al., J. Agric. Food Chem. 4, 236 (1956) DOI. Configuration of isomers: T. R. Fukuto et al., J. Org. Chem. 26, 4620 (1961) DOI. Metabolism and degradn: K. I. Beynon et al., Residue Rev. 47, 55 (1973) PubMed. Toxicity study: T. B. Gaines, Toxicol. Appl. Pharmacol. 14, 515 (1969) DOI PubMed. GC-MS determn in animal tissue: W. J. Allender, J. Keegan, J. Chromatogr. 609, 315 (1992) DOI PubMed.
Properties
Yellow liquid. d420 1.25. nD20 1.4494. bp1 106-107.5°. Poisonous. Misc with
water, acetone, benzene, carbon tetrachloride, chloroform, ethyl and
isopropyl alcohols, toluene and xylene. One gram dissolves in 20
ml carbon disulfide and 20 ml kerosene. Practically insol in hexane.
LD50 in female, male rats (mg/kg): 3.7, 6.1 orally; 4.2, 4.7 dermally (Gaines).Caution
Potential symptoms of overexposure
are miosis; rhinorrhea; headache; tight chest, wheezing, laryngeal
spasm, salivation and cyanosis; anorexia, nausea, vomiting, abdominal
cramps and diarrhea; paralysis; ataxia, convulsions; low blood pressure,
cardiac irregularities; irritation of skin, eyes and respiratory system.
See NIOSH Pocket Guide to Chemical
Hazards (DHHS/NIOSH 97-140, 1997) p 252.Use
Insecticide.