6509. Nickel Formate

Nomenclature

CAS number: 3349-06-2
C2H2NiO4; mol wt 148.73.
C 16.15%, H 1.36%, Ni 39.46%, O 43.03%.
Ni(HCOO)2.

Description and references

Prepd by reaction of formic acid with Ni: Johnson, US 2576072 (1951 to Harshaw Chemical); with NiCO3: Bircumshaw, Edwards, J. Chem. Soc. 1950, 1800.

Derivative

Dihydrate.

Properties

Fine, green, monoclinic crystals. Becomes anhydr on careful heating to 130-140°; decomposes at 180-200° yielding Ni, CO, CO2, H2, H2O, CH4. d20.2 2.154. Moderately sol in water. Practically insol in alc, formic acid.

Use

Manuf of Ni; prepn of Ni catalysts for organic reactions, particularly hydrogenation catalysts.