7154. Perchloryl Fluoride

Nomenclature

CAS number: 7616-94-6
ClFO3; mol wt 102.45.
Cl 34.61%, F 18.54%, O 46.85%.

Description and references

Reviews: Downs, Adams in Comprehensive Inorganic Chemistry vol. 2, J. C. Bailar, Jr. et al., Eds. (Pergamon Press, Oxford, 1973) pp 1391-1393; Christe, Schack in Adv. Inorg. Chem. Radiochem. 18, 319-398.

Chemical structure

Properties

Characteristic sweet odor. Usually stored in cylinders as liquid under pressure. mp -147.7°. bp -46.7°. d20 (liq) 1.434. Critical temp 95.2°. Crit pressure 53 atm. Crit density: 0.637. Heat of vaporization 4.6 kcal/mol. Trouton constant: 20.4. Dipole moment 0.03. Heat of formation of gas at 25° -5.12 kcal/mol. Sp heat of liquid: 0.229 cal/g/°C at -40°; 0.290 at +50°. Does not corrode base metals when anhydr. Shows the greatest resistance to electrical breakdown known for any gas. Handle with caution. Do not bring in direct contact with reducing agents, alcohols, etc.: Chem. Eng. News 37, 60 (1959). Explosions have occurred.

Caution

Potential symptom of overexposure is respiratory system irritation; direct contact with liquid may cause frostbite. See NIOSH Pocket Guide to Chemical Hazards (DHHS/NIOSH 97-140, 1997) p 246. May cause methemoglobinemia, cyanosis, alveolar edema, bronchopneumonia. See Patty's Industrial Hygiene and Toxicology vol. 2F, G. D. Clayton, F. E. Clayton, Eds. (John Wiley & Sons, New York, 4th ed., 1994) p 4478.

Use

In organic synthesis to introduce fluorine atoms into organic molecules. As oxidizing agent; insulator for high voltage systems.