Prepn: Gray, Maxson, Inorg. Synth.2, 147 (1946). Review: Payne, “The Chemistry of Phosphorus Halides” in Topics in Phosphorus Chemistryvol.
4, M. Grayson, E. J. Griffith, Eds. (Interscience, New York,
1967) pp 85-155.
Properties
Colorless, fuming liquid; very penetrating odor.
d15 2.85. mp -41.5°. bp 173.2°. Vapor pressure:
10 mm (48°). Dissolved and dec by water or alc; sol in acetone,
carbon disulfide. Corrosive. Keep tightly
closed.