Description and references
Best prepd from the elements in liq ammonia:
Klemm et al., Z. Anorg. Allg.
Chem. 241, 281 (1939); Feher in Handbook of Preparative Inorganic Chemistry vol. 1, G. Brauer, Ed. (Academic Press, New York, 2nd
ed., 1963) pp 360-361.
Derivative
Pentahydrate.
Properties
Colorless rhombs. Odor of hydrogen sulfide.
Discolors upon exposure to light and air (yellow to yellowish red).
mp 60°.
Spontaneously combustible. Freely sol in
water, alc, glycerol. Insol in ether. Densities
of aq solutions at 25° (calcd as % K
2S.5H
2O):
1.82%: 1.009; 10.90%: 1.049; 21.80%: 1.100; 29.07%: 1.136; 39.97%: 1.192; 50.88%: 1.250; 81.77%: 1.432. Aq solns are very caustic and prone to decompn.
See the hydrolysis reactions
under Sodium Sulfide.