Prepn: S. Gabriel, G. Pinkus, Ber.26, 2197 (1893); P. Brandes,
C. Stoehr, J. Prakt. Chem. [2]54, 481 (1896). See also:BeilsteinXXIII, 91 (1936). Crystal
structure: G. De With et al.,Acta Crystallogr.B32, 3178 (1976).
Properties
Crystals or wax-like solid. Strong pyridine-like
odor. d461 1.031; mp 53°; bp 115-118°; nD61 1.4953. Freely sol in water, alcohol,
ether. Volatile with steam.