12-10057. Vanadium Tetrafluoride [Archived]

Nomenclature

CAS number: 10049-16-8
F4V; mol wt 126.94.
F 59.87%, V 40.13%.
VF4.

Description and references

Prepd from VCl4 and HF or from the elements: Ruff, Lickfett, Ber. 44, 2539 (1911); Cavell, Clark, J. Chem. Soc. 1962, 2692; Kwasnik in Handbook of Preparative Inorganic Chemistry vol. 1, G. Brauer, Ed. (Academic Press, New York, 2nd ed., 1963) pp 252-253.

Properties

Bright lime-green powder; very hygroscopic; hydrolyzes to form a brown powder and eventually a blue paste. d 3.15. Sublimes at 100-120° in a vacuum. Also disproportionates to VF3 and VF5 at 100-120° in a vacuum. Freely sol in water with blue color, in acetone deep green, in glacial acetic acid blue green. Sparingly sol in alc, chloroform, SO2Cl2. May be stored in sealed iron or copper vessels.

Status

This monograph has been retired and is no longer subject to revision or update.