Prepd from red phosphorus and aluminum powder: White, Bushey, J. Am. Chem. Soc. 66, 1666 (1944); Inorg. Synth. 4, 23 (1953); Montignie, Bull. Soc. Chim. Fr. 1946, 276; from Al and Zn2P3: Wang et al., J. Inorg. Nucl. Chem. 25, 326 (1963). Use as insecticidal fumigant: W. Freyberg, W. Haupt, US 2117158 (1938 to Freyberg).