2135. Chlorodibromomethane

Nomenclature

CAS number: 124-48-1
Dibromochloromethane; chlorobromoform; monochlorodibromomethane; DBCM; NCI-C55254.
CHBr2Cl; mol wt 208.28.
C 5.77%, H 0.48%, Br 76.73%, Cl 17.02%.

Description and references

Trihalomethane contaminant found in chlorinated water. Prepn: O. Jacobsen, R. Neumeister, Ber. 15, 599 (1882); M. Fedorynski et al., Synth. Commun. 7, 287 (1977). Toxicity studies: F. J. Bowman et al., Toxicol. Appl. Pharmacol. 44, 213 (1978); Y. Aida et al., J. Toxicol. Sci. 17, 119 (1992). Review of toxicology and human exposure: Toxicological Profile for Bromoform and Dibromochloromethane (PB2006-100001, 2005) 273 pp. Review of carcinogenic risk: IARC Monographs 52, 243-268 (1991).

Properties

Liquid. bp 121.3-121.8° (Fedorynski); also reported as bp 123-125° (Jacobsen). d15 2.4450. nD20 1.5471. Sol in ethanol, ether, acetone. LD50 in male, female rats (mg/kg): 370, 760 orally (Aida); in male, female mice (mg/kg): 800, 1200 by gavage (Bowman).

Use

Chemical reagent/intermediate in organic synthesis.