Nomenclature
CAS number: 122-03-2
4-(1-Methylethyl)benzaldehyde;
p-isopropylbenzaldehyde; cuminal; cumaldehyde.
C
10H
12O; mol wt 148.20.
C 81.04%, H 8.16%, O 10.80%.
Description and references
Constituent of eucalyptus, myrrh, cassia, cumin,
and other essential oils; prepared synthetically from p-isopropylbenzoyl chloride. Alternate synthesis by formylation of
isopropylbenzene under pressure: Crounse, J. Am. Chem. Soc. 71, 1263 (1949). Toxicity
study: P. M. Jenner et al., Food
Cosmet. Toxicol. 2, 327 (1964).
Properties
Colorless to yellowish, oily liq; strong persistent
odor; acrid, burning taste. d20 0.978. bp760 235-236°; bp35 131-135°. nD20 1.5301. Practically insol in water. Sol in alc, ether. LD50 orally in rats:
1390 mg/kg (Jenner).Derivative
Thiosemicarbazone.
Nomenclature
CAS number: 3811-20-9
SHCH-58.
C
11H
15N
3S; mol wt 221.32.
C 59.70%, H 6.83%, N 18.99%, S 14.49%.
Description and references
Prepn: P. P. T. Sah, T. C. Daniels, Rec. Trav. Chim. 69, 1545 (1950);
J. Bernstein et al., J. Am. Chem.
Soc. 73, 906 (1951).
Properties
Stout platelets from methanol, mp 147°. Practically insol in water.
Moderately sol in alc.Use
In perfumery.