2849. Decamethylene Glycol
Nomenclature
CAS number: 112-47-0
1,10-Decanediol. C10H22O2; mol wt 174.28.
C 68.92%, H 12.72%, O 18.36%.
Description and references
Prepd by the reduction of dimethyl or diethyl sebacate with sodium and ethyl alcohol: Bouveault, Blanc, Compt. Rend. 137, 329 (1903); Bull. Soc. Chim. [3] 31, 1205 (1904); DE 164294; Frdl. 8, 1260 (1905); Chuit, Helv. Chim. Acta 9, 264 (1926); Manske, Org. Synth. 14, 20 (1934). By catalytic hydrogenation of sebacic esters: Folkers, Adkins, J. Am. Chem. Soc. 54, 1146 (1932).
Properties
Needles from water or dil alcohol. mp 74°. bp20 192°; bp11 179°; bp8 170°. Freely sol in alcohol, warm ether; almost insol in petr ether and water.Derivative
Diethyl ether.Nomenclature
CAS number: 5895-59-0
1,10-Diethoxydecane. C14H30O2; mol wt 230.39.
C 72.98%, H 13.12%, O 13.89%.