Nomenclature
CAS number: 90-00-6
Phlorol;
o-ethylphenol.
C
8H
10O; mol wt 122.16.
C 78.66%, H 8.25%, O 13.10%.
Description and references
Prepn: W. Suida, S. Plohn, Monatsh. Chem. 1, 175 (1880).
Purification and properties: D. P. Biddiscombe et al., J. Chem. Soc. 1963, 5764. Colorimetric determn of isomeric purities in reagent grade
chemicals: I. M. Jakovljevic, R. H. Bishara, J. Chromatogr. 192, 425 (1980). Thermolytic
reactions: P. Zhou, B. L. Crynes, Ind. Eng.
Chem. Process Des. Dev. 25, 898 (1986). Decomposition
and oxidation of aqueous solns: C. J. Martino, P. E. Savage, Ind. Eng. Chem. Res. 38, 1775
(1999).
Properties
Colorless liquid; phenol odor. Cooling the liquid
to -30° gives a metastable cryst form, mp about -28°; when kept for 24-48 hrs, this changes
to the stable cryst form, mp -3.4°. fp -3.31 ± 0.01° for repurified sample. bp760 204.52°. d20 1.01885 ± 0.00001; d25 1.01459; d30 1.01033 ±
0.00001 (g/ml). Practically insol in water. Freely sol
in alcohol, benzene, glacial acetic acid.Use
Starting material and intermediate for pharmaceutical
and agricultural chemicals.