Prepn: GB902292; F. H. Lincoln et al.,US3499016 (1962, 1970 both to Upjohn). Prepn of the 21-acetate:
J. A. Edwards et al.,J. Am. Chem.
Soc.81, 3156 (1959); 82, 2318 (1960).
Derivative
21-Acetate.
C24H30F2O6; mol wt 452.49.
C 63.70%, H 6.68%, F 8.40%, O 21.22%.
Properties
Crystals from acetone + hexane, mp 260-264°. [α]D +91°. uv max (ethanol): 237 nm
(log ε 4.16).