4167. Fluoroacetic Acid

Nomenclature

CAS number: 144-49-0
2-Fluoroacetic acid; cymonic acid; fluoroethanoic acid; gifblaar poison; monofluoroacetic acid; FAA.
C2H3FO2; mol wt 78.04.
C 30.78%, H 3.87%, F 24.34%, O 41.00%.

Description and references

Toxic constituent of the poisonous South African plant, Dichapetalum cymosum (Hook.) Engl., Dichapetalaceae, commonly known as gifblaar (“poison leaf”). Also contained in other poisonous plant species. Metabolically converted to fluorocitrate which inhibits the tricarboxylic acid cycle resulting in cellular hypoxia. Prepn via methyl ester: F. Swarts, Bull. Soc. Chim. [3] 15, 1134 (1896); B. C. Saunders, G. J. Stacey, J. Chem. Soc. 1948, 1773 DOI; by fluorination of disodium malonate: V. Grakauskas, J. Org. Chem. 34, 2446 (1969) DOI. Isoln from gifblaar: J. S. C. Marais, Onderstepoort J. Vet. Res. 20, 67 (1944). Mechanism of toxicity: R. A. Peters, Endeavour 13, 147 (1954). Determn in biological samples using HS-SPME: F. Sporkert et al., J. Chromatogr. B 772, 45 (2002) DOI PubMed. Review of properties and use: A. J. Elliott in Kirk-Othmer Encyclopedia of Chemical Technology vol. 11 (Wiley-Interscience, New York, 4th ed., 1994) pp 544-550. Review of toxicology: N. V. Goncharov et al., J. Appl. Toxicol. 26, 148-161 (2006) DOI PubMed.

Chemical structure

Properties

Colorless needles, mp 31-32°. bp 165°. pKa 2.59. d 1.37. Sol in water. Burns with a green flame.

Derivative

Sodium salt.

Nomenclature

CAS number: 62-74-8
Sodium fluoroacetate; compound 1080.
C2H2FNaO2; mol wt 100.02.
C 24.02%, H 2.02%, F 18.99%, Na 22.99%, O 31.99%.

Properties

Hygroscopic white solid. mp 200-202° (dec when heated above mp). Soly at 25° (g/100g): water 111, methanol 5, ethanol 1.4, acetone 0.04, carbon tetrachloride 0.004.

Derivative

Methyl ester.

Nomenclature

CAS number: 453-18-9
Methyl fluoroacetate; MFA.
C3H5FO2; mol wt 92.07.
C 39.14%, H 5.47%, F 20.63%, O 34.75%.

Properties

Mobile liquid, fp 32°. Practically odorless or faint, fruit-like odor. d420 1.1744; d415 1.1613. nD20 1.3679. bp 104.5°. Sol in water; slightly sol in petr ether. LD50 in rabbits, mice (mg/kg): 0.25 i.v.; 7-10 s.c. (Saunders, Stacey).

Derivative

Ethyl ester.

Nomenclature

CAS number: 459-72-3
C4H7FO2; mol wt 106.10.
C 45.28%, H 6.65%, F 17.91%, O 30.16%.

Properties

Liq, odor of ethyl acetate. d20.5 1.0926. bp758 121.6°. nD20.5 1.3767. Sol in water.

Caution

Fluoroacetates are highly toxic. Potential symptoms of overexposure are vomiting; apprehension; clonic-tonic convulsions; depression; loss of consciousness; metabolic acidosis; hypotension; cardiac arrhythmias; respiratory failure; hypocalcemia; renal failure; death (Goncharov).

Use

Rodenticide.