5020. Iodine Trichloride

Nomenclature

CAS number: 865-44-1
Cl3I; mol wt 233.26.
Cl 45.60%, I 54.40%.
ICl3.

Description and references

Prepd by adding finely powdered iodine to an excess of liq chlorine, which is then boiled away: Thomas, Depuis, Compt. Rend. 143, 282 (1906); Booth, Morris, Inorg. Synth. 1, 167 (1939). Alternate process: Birk, Angew. Chem. 41, 751 (1928); Z. Anorg. Allg. Chem. 172, 399 (1928); Wilke-Drfurt, Wolff, ibid. 185, 333 (1930).

Properties

Long yellow or brownish needles or fluffy powder. Pungent, irritating odor. Corrosive to human skin. Must be stored in well closed amber glass bottles, preferably in refrigerator. d4 3.203. mp ≈33°. Volatile at room temp. mp 101° at 16 atm (pressure of its satd vapor). A pressure of 1 atm is reached at 64°. Complete decompn into ICl and Cl2 at 77°. Generally used as a 20 to 35% soln in concd HCl.

Caution

Concd solns are strongly irritating.

Use

Chlorinating and oxidizing agent.

Therapeutic Category

Anti-infective (topical).

Keywords

Antiseptic/Disinfectant; Halogens/Halogen Containing Compounds