Nomenclature
CAS number: 60-82-2
3-(4-Hydroxyphenyl)-1-(2,4,6-trihydroxyphenyl)-1-propanone; 2′,4′,6′-trihydroxy-3-(
p-hydroxyphenyl)propiophenone; β-(
p-hydroxyphenyl)phloropropiophenone; β-(
p-hydroxyphenyl)-2,4,6-trihydroxypropiophenone.
C
15H
14O
5; mol wt 274.27.
C 65.69%, H 5.14%, O 29.17%.
Description and references
The aglucon of phlorizin, q.v. From root bark of apple trees: Rochleder, J. Prakt. Chem. 98, 205 (1866).
Structure: Seshadri, Annu. Rev. Biochem. 20, 495 (1951). Synthesis: Fischer, Nouri, Ber. 50, 611 (1917); Rosenmund,
Rosenmund, ibid. 61B, 2608 (1928); Shinoda et al., J. Pharm. Soc. Jpn. 49, 797 (1929); Johnston, US 2789995 (1957 to Union Carbide).
Properties
Needles from dil alcohol, dec 262°. Absorption
spectrum: Lambrechts, Arch. Int. Physiol. 44, Suppl., 1-39 (1937). Freely sol in alc, methanol,
acetone; sol in alkalies in hot glacial acetic acid; very sparingly
sol in benzene, chloroform. Practically insol in water, ether, the
soly being increased by addition of alcohol.