9320. Thioacetic Acid

Nomenclature

CAS number: 507-09-5
Ethanethioic acid; thiolacetic acid; thiacetic acid.
C2H4OS; mol wt 76.12.
C 31.56%, H 5.30%, O 21.02%, S 42.12%.
CH3COSH.

Description and references

Prepn by distilling glacial acetic acid with phosphorus pentasulfide: Kekulé, Ann. 90, 309 (1854); from acetic anhydride and hydrogen sulfide: Ellingboe, Org. Synth. 31, 105 (1951).

Properties

Yellow liquid; pungent odor. Flammable. d410 1.075; bp 93°. Not solidified at 17°. Sol in water, particularly hot; very sol in alcohol.