Nomenclature
CAS number: 528-44-9
1,2,4-Benzenetricarboxylic acid; 1,2,4-tricarboxybenzene.
C
9H
6O
6; mol wt 210.14.
C 51.44%, H 2.88%, O 45.68%.
Description and references
Obtained by oxidation of coal with nitric acid:
Grosskinsky, Glueckauf 88, 376 (1952), C.A. 46, 7731 (1952); by oxidation of β-indancarboxylic acid with nitric
acid: Braun et al., Ber. 53, 1160 (1920). Manuf by oxidation of pseudocumene:
Backlund, US 3009953 (1961 to Union Oil of Calif.).
Properties
Crystals from acetic acid or dilute alcohol. mp 218-220° (also reported 229-234° dec). Solubilities at 25° in g/100
g solvent: carbon tetrachloride 0.004; ligroin 0.03; mixed xylenes
0.006; dimethylformamide 31.3; ethyl acetate 1.7; acetone 7.9; water
2.1; ethanol 25.3. Practically insol in chloroform, benzene, carbon
disulfide.Use
Intermediate in the prepn of resins, plasticizers,
dyes, inks, adhesives.