Nomenclature
CAS number: 127-65-1
N-Chloro-4-methylbenzenesulfonamide sodium salt
(1:1); (
N-chloro-
p-toluenesulfonamido)sodium; sodium
p-toluenesulfonchloramide; chloramine; tosylchloramide sodium; Chlorazene (WPC); Euclorina (Bracco); Halamid (Akzo).
C
7H
7ClNNaO
2S; mol wt 227.64.
C 36.93%, H 3.10%, Cl 15.57%, N 6.15%, Na 10.10%, O 14.06%,
S 14.09%.
Description and references
Prepd via p-toluenesulfonamide:
Chattaway, J.
Chem. Soc. 87, 145 (1905); Inglis, J. Soc. Chem. Ind. London 37, 288 (1918); F. J. Welcher, Organic Analytical Reagents vol. 4 (Van Nostrand, New York, 1948) pp 316-320. Reviews of synthetic
applications: M. M. Campbell, G Johnson, Chem. Rev. 78, 65-79 (1978); G. Agnihotri, Synlett 2005, 2857-2858.
Derivative
Trihydrate.
Nomenclature
CAS number: 7080-50-4
C
7H
7ClNNaO
2S.3H
2O; mol wt 281.69.
C 29.85%, H 4.65%, Cl 12.59%, N 4.97%, Na 8.16%, O 28.40%, S
11.38%.
Properties
Prisms. Loses water on drying. Dec slowly on
exposure to air. Keep well closed. Corrosive Fairly sol in water. Practically insol in benzene, chloroform,
ether. Dec by alc.Detection of bromate and halogens. Source of halonium
ions and nitrogen anions in organic synthesis.
Antibacterial.
Antiseptic (topical).