Prepn: Dekker, Todd, Nature 166, 557 (1950); Brown et al., J. Chem. Soc. 1958, 3035; Prystas et al., Collect. Czech. Chem. Commun. 28, 3140 (1963); Smejkal et al., ibid. 31, 291 (1966). Conformation: Rahman, Wilson, Nature 232, 333 (1971).
Prepn: Prystas et al., loc. cit.